V. A. D'yakonov, A. A. Makarov, L. U. Dzhemileva, E. N. Andreev, U. M. Dzhemilev, “The first total synthesis of lembehyne B”, Mendeleev Commun., 27:2 (2017), 122

Эта публикация цитируется в 13 статьях

Communications

The first total synthesis of lembehyne B

V. A. D'yakonov, A. A. Makarov, L. U. Dzhemileva, E. N. Andreev, U. M. Dzhemilev

Institute of Petrochemistry and Catalysis, Ufa Federal Research Centre of the Russian Academy of Sciences, Ufa, Russian Federation

Аннотация: The total synthesis of lembehyne B was accomplished in five steps in 51% total yield. The cross-cyclomagnesiation of two allenic components, nonadeca-1,2-diene and pentadeca-13,14-dien-1-ol tetrahydropyranyl ether, with EtMgBr in the presence of Mg and Cp₂TiCl₂ catalyst (10 mol%) was used in the key step of the synthesis.

Язык публикации: английский

DOI: 10.1016/j.mencom.2017.03.004

	*Дополнительные материалы:*
		Supplementary_data_1.pdf	532.0 Kb