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Fizika Tverdogo Tela, 2019 Volume 61, Issue 6, Pages 1190–1196 (Mi ftt8800)

Polymers

A study of solid phase transition kinetics in the tetracosane Ñ$_{24}$Í$_{50}$ with the help of high resolution synchrotron X-ray powder diffraction

V. A. Marikhina, P. V. Dorovatovskiib, Ya. V. Zubavichusc, M. V. Baidakovaa, E. M. Ivan'kovad, L. P. Myasnikovaa

a Ioffe Institute, St. Petersburg
b National Research Centre "Kurchatov Institute", Moscow
c Boreskov Institute of Catalysis SB RAS, Novosibirsk
d Institute of Macromolecular Compounds, Russian Academy of Sciences, St. Petersburg

Abstract: Using the small-angle synchrotron X-ray diffraction method at the research facility “BELOK” of the Kurchatov synchrotron radiation source at the NRC Kurchatov Institute, it was shown that the first-order solid phase transition in tetracosane Ñ$_{24}$Í$_{50}$ passes according to a heterogeneous mechanism in a narrow temperature range $\Delta T\sim$ K in accordance with the theory of diffuse phase transitions.

Received: 15.01.2019
Revised: 15.01.2019
Accepted: 15.01.2019

DOI: 10.21883/FTT.2019.06.47698.355


 English version:
Physics of the Solid State, 2019, 61:6, 1128–1135

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