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Fizika Tverdogo Tela, 2017 Volume 59, Issue 9, Pages 1673–1679 (Mi ftt9449)

This article is cited in 3 papers

Superconductivity

Mechanism of the formation of structure during high-temperature annealing of MgB$_{2}$ bulk samples deformed under pressure

E. I. Kuznetsova, M. V. Degtyarev, Yu. V. Blinova, S. V. Sudareva, Yu. N. Akshentsev, V. P. Pilyugin

Institute of Metal Physics, Ural Division of the Russian Academy of Sciences, Ekaterinburg

Abstract: MgB$_{2}$ superconductors subjected to deformation under pressure on Bridgeman anvils and subsequent annealings at 800 and 950$^\circ$C were investigated by X-ray diffraction, scanning electron microscopy, and microanalysis. It was shown that at these temperatures crystals of MgB$_{2}$ phase along the residual boron dissolute in the residual liquid magnesium with the formation of both dense and loose areas of MgB$_{2}$ phase. The latter has a negative influence on critical current. At the same time, after these treatments, the samples become more uniform by the phase and chemical composition.

Received: 14.03.2017

DOI: 10.21883/FTT.2017.09.44835.076


 English version:
Physics of the Solid State, 2017, 59:9, 1695–1701

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