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Zhurnal Tekhnicheskoi Fiziki, 2020 Volume 90, Issue 4, Pages 627–636 (Mi jtf5338)

This article is cited in 6 papers

Solids

Atomic disordering and BCC $\to$ FCC transformation in the Heusler compound Ni$_{54}$Mn$_{20}$Fe$_{1}$Ga$_{25}$ subject to high-pressure torsional megaplastic deformation

V. G. Pushinab, N. N. Kuranovaab, E. B. Marchenkovaa, A. V. Pushinab

a Institute of Metal Physics, Ural Division of the Russian Academy of Sciences, Ekaterinburg
b Ural Federal University named after the First President of Russia B. N. Yeltsin, Ekaterinburg

Abstract: The Heusler compound with the $L$2$_1$ Ni$_{54}$Mn$_{20}$Fe$_{1}$Ga$_{25}$ structure subject to high-pressure torsional megaplastic deformation was first systematically studied by in situ methods of X-ray phase analysis and transmission and scanning electron microscopy. It was established that the torsional shear deformation at room temperature reduces the polycrystalline structure of the compound to a nanocrystalline and partially amorphous state. It was revealed that, as the pressure increases from 3 to 5 GPa and the degree of deformation increases from 2 to 5 revolutions, total atomic disordering and sequential structural-phase transformation according to the scheme $B$2(BCC) $\to$ $A$2(BCC) $\to$ $A$1(FCC) occur. It is shown that annealing at a temperature of 570 K and below causes devitrification of the amorphous phase and annealing at a temperature of 620 K and above causes the restoration of the $L$2$_1$ structure. The dimensional effect of suppressing the thermoelastic martensitic transformation is revealed in the nanostructured austenitic $L$2$_1$ alloy with grains smaller than 80 nm when cooled to 120 K. The capability of the thermoelastic martensitic transformation and of the shape memory is restored in a submicrocrystalline ultrafine-grained alloy after its recrystallization annealing at temperatures above 600 K.

Keywords: alloys of Heusler, megaplastic deformation, nanostructure, atomic disordering, amorphization, devitrification, ultrafine grained structure, thermoelastic martensitic transformation, physical properties.

Received: 30.09.2019
Revised: 30.09.2019
Accepted: 21.10.2019

DOI: 10.21883/JTF.2020.04.49088.318-19


 English version:
Technical Physics, 2020, 65:4, 602–611

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