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Zhurnal Tekhnicheskoi Fiziki, 2022 Volume 92, Issue 9, Pages 1460–1466 (Mi jtf7449)

Experimental instruments and technique

Determination of the massive component contribution from the analysis of line shape distortions in diffraction spectra for nanocomposite materials

O. A. Alekseevaab, A. A. Naberezhnovc, Georges-Ivo Ekossed

a Peter the Great St. Petersburg Polytechnic University, 195251 St. Petersburg, Russia
b Tomsk State University of Control Systems and Radioelectronics, 634050 Tomsk, Russia
c Ioffe Institute, 194021 St. Petersburg, Russia
d University of Venda, University Road, 0950 Thohoyandou, South Africa

Abstract: Using the analysis of the elastic lines distortions of the diffraction spectra with the involvement of the high order central moments of the distribution, the sensitivity of the developed technique to the presence of an admixture of a bulk component in nanocomposite materials was estimated. Cases for the main types of instrumental resolution functions of diffractometers and functions describing the response from materials embedded in the pore space of nanomatrices such as SBA-15, MCM-41, MCM-48, etc. are considered.

Keywords: porous matrices, diffraction, resolution function, nanocomposite materials, elastic peak line shape, higher central moments of distribution.

Received: 10.03.2022
Revised: 10.03.2022
Accepted: 17.05.2022

DOI: 10.21883/JTF.2022.09.52939.50-22



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