I. G. Mamedov, V. N. Khrustalev, P. V. Dorovatovskii, F. N. Naghiev, A. M. Maharramov, “Efficient synthesis of new tricyclic pyrano[3,2-<i>c</i>]pyridine derivatives”, Mendeleev Commun., 2019, Volume 29, Issue 2,Pages <nobr>232

This article is cited in 12 papers

Communications

Efficient synthesis of new tricyclic pyrano[3,2-c]pyridine derivatives

I. G. Mamedov^a, V. N. Khrustalev^bc, P. V. Dorovatovskii^c, F. N. Naghiev^a, A. M. Maharramov^a

^a Department of Chemistry, Baku State University, Baku, Azerbaijan
^b Peoples Friendship University of Russia (RUDN University), Moscow, Russian Federation
^c National Research Centre 'Kurchatov Institute', Moscow, Russian Federation

Abstract: Reaction between arylidenemalononitriles and acetoacetanilide in the presence of piperazine hydrate in methanol at room temperature affords new tricyclic pyrano[3,2-c]pyridine derivatives of (rac-1S*,2R*,3R*,7R*,8R*,11R*)-2,11-diaryl-4,10-diimino-8-methyl-5-phenyl-6-oxo-9-oxa-5-azatricyclo-[5.3.1.0^3,8]undecane-1,3-dicarbonitrile family in yields of 55–84%. The molecular structures of the products were confirmed by X-ray crystallography and NMR spectroscopy.

Language: English

DOI: 10.1016/j.mencom.2019.03.040

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