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JOURNALS // Mendeleev Communications // Archive

Mendeleev Commun., 2016 Volume 26, Issue 4, Pages 323–325 (Mi mendc2201)

This article is cited in 12 papers

Communications

A new synthesis of a nitroimino-containing 1,2,4-triazin-5-one from 3-bromo-3-nitropropenoates

V. M. Berestovitskayaa, O. Yu. Ozerovaa, T. P. Efimovaa, V. V. Gurzhiyb, T. A. Novikovaa

a Department of Chemistry, Russian State Pedagogical University, St. Petersburg, Russian Federation
b Department of Geology, St. Petersburg State University, St. Petersburg, Russian Federation

Abstract: Reaction of 1-amino-2-nitroguanidine with alkyl 3-bromo-3-nitropropenoates affords 3-nitroimino-6-nitromethyl-4,5-dihydro-(2H)-1,2,4-triazin-5-one, whose structure was characterized by IR, UV, NMR spectroscopy and X-ray single crystal analysis.

Language: English

DOI: 10.1016/j.mencom.2016.07.019



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