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JOURNALS // Mendeleev Communications // Archive

Mendeleev Commun., 2016 Volume 26, Issue 5, Pages 375–377 (Mi mendc2217)

This article is cited in 3 papers

Communications

Tandem AN–AN reactions in the synthesis of tetrahydrothiazolo[4,5-e][1,2,4]triazines

N. N. Mochulskayaab, P. A. Slepukhinab, V. N. Charushinab, M. I. Kodessab

a Department of Chemistry, Ural Federal University, Ekaterinburg, Russian Federation
b I.Ya. Postovsky Institute of Organic Synthesis, Ural Branch of the Russian Academy of Sciences, Ekaterinburg, Russian Federation

Abstract: Reaction of 3-aryl-1,2,4-triazines with S,N-dinucleophilic N-(het)arylthioureas in acetic anhydride at room temperature affords the cyclization products, tetrahydrothiazolo[4,5-e]-[1,2,4]triazines in good yields. The structure of the heterocyclic system thus formed was confirmed by X-ray diffraction analysis.

Language: English

DOI: 10.1016/j.mencom.2016.09.002



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