A. O. Terent'ev, O. M. Mulina, D. A. Pirgach, M. A. Syroeshkin, A. P. Glinuskin, G. I. Nikishin, “Electrochemical synthesis of sulfonamides from arenesulfonohydrazides or sodium <i>p</i>-methylbenzenesulfinate and amines”, Mendeleev Commun., 2016, Volume 26, Issue 6,Pages <nobr>538

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Communications

Electrochemical synthesis of sulfonamides from arenesulfonohydrazides or sodium p-methylbenzenesulfinate and amines

A. O. Terent'ev^abc, O. M. Mulina^a, D. A. Pirgach^ab, M. A. Syroeshkin^a, A. P. Glinuskin^c, G. I. Nikishin^a

^a N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation
^b D.Mendeleev University of Chemical Technology of Russia, Moscow, Russian Federation
^c All-Russian Research Institute of Phytopathology, Bol'shiye Vyazemy, Moscow Region, Russian Federation

Abstract: An efficient electrochemical synthesis of sulfonamides (yields 56–98%) from arenesulfonohydrazides or sodium p-methylbenzenesulfinate and amines was performed in an undivided cell with graphite anode and iron cathode in MeCN–H₂O medium using halides as redox mediators and supporting electrolytes.

Language: English

DOI: 10.1016/j.mencom.2016.11.027

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