V. I. Isaeva, A. L. Tarasov, V. V. Chernyshev, L. M. Kustov, “Control of morphology and size of microporous framework MIL-53(Al) crystals by synthesis procedure”, Mendeleev Commun., 2015, Volume 25, Issue 6,Pages <nobr>466

This article is cited in 30 papers

Communications

Control of morphology and size of microporous framework MIL-53(Al) crystals by synthesis procedure

V. I. Isaeva^a, A. L. Tarasov^a, V. V. Chernyshev^b, L. M. Kustov^ab

^a N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation
^b Department of Chemistry, M.V. Lomonosov Moscow State University, Moscow, Russian Federation

Abstract: Two methods for the preparation of microporous phenylenecarboxylate framework MIL-53(Al), solvothermal high-pressure procedure and synthesis at atmospheric pressure, were compared in respect of crystal morphology and size. Lower reaction time and temperature featured microwave method providing nanocrystallites of homogeneous distribution in shape and size.

Language: English

DOI: 10.1016/j.mencom.2015.11.023