Mendeleev Commun., 2014 Volume 24, Issue 4, Pages 211–213
(Mi mendc2526)
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6 papers
Communications Radical reaction of C70 Cl10 with P(OEt)3 : isolation and characterization of C70 [P(O)(OEt)2 ]n n n = 1, 2) E. A. Khakina a ,
A. A. Yurkova a ,
A. V. Novikov ab ,
N. P. Piven' c ,
A. V. Chernyak ad ,
A. S. Peregudov e ,
P. A. Troshin a a Institute of Problems of Chemical Physics, Russian Academy of Sciences, Chernogolovka, Moscow Region, Russian Federation b Department of Fundamental Physical and Chemical Engineering, M.V. Lomonosov Moscow State University, Moscow, Russian Federation c Institute of Energy Problems for Chemical Physics RAS (Branch), Chernogolovka, Moscow region, Russian Federation
d Scienific Center in Chernogolovka, Russian Academy of Sciences, Chernogolovka, Moscow Region, Russian Federation e A.N. Nesmeyanov Institute of Organoelement Compounds of Russian Academy of Sciences, Moscow, Russian Federation Abstract:
The Arbuzov-type reaction of chlorofullerene C
70 Cl
10 with P(OEt)
3 leads to the formation of C
70 [P(O)(OEt)
2 ]H and C
70 [P(O)(OEt)
2 ]
2 H
2 , whose molecular structures were determined using ESI mass spectrometry in combination with 1D and 2D NMR spectroscopy.
Language: English
DOI:
10.1016/j.mencom.2014.06.007
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