D. V. Shamshurin, I. V. Zavarzin, V. N. Yarovenko, E. I. Chernoburova, M. M. Krayushkin, Yu. V. Volgin, E. N. Shapovalova, P. N. Nesterenko, O. A. Shpigun, “Thiooxamide chiral stationary phase for liquid chromatography”, Mendeleev Commun., 2005, Volume 15, Issue 4,Pages <nobr>143–145</nobr>

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Mendeleev Commun., 2005 Volume 15, Issue 4, Pages 143–145 (Mi mendc3717)

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Thiooxamide chiral stationary phase for liquid chromatography

D. V. Shamshurin^a, I. V. Zavarzin^b, V. N. Yarovenko^b, E. I. Chernoburova^b, M. M. Krayushkin^b, Yu. V. Volgin^a, E. N. Shapovalova^a, P. N. Nesterenko^a, O. A. Shpigun^a

^a Department of Chemistry, M.V. Lomonosov Moscow State University, Moscow, Russian Federation
^b N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation

Abstract: A new chiral stationary phase was prepared by reaction of aminopropylsilica with N-(α-phenylethyl)chloroacetamide in the presence of sulfur and used for the high performance liquid-chromatographic separation of 1,1′-binaphthyl-2,2′-diol and Tröger's base enantiomers.

Language: English

DOI: 10.1070/MC2005v015n04ABEH002110

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