D. B. Nilov, V. G. Granik, “Synthesis and properties of benzo[b]thiopheno[2,3-d]-1,3,2λ5-diazaphosphinane-2-thione derivatives”, Mendeleev Commun., 2003, Volume 13, Issue 2,Pages 78

This article is cited in 9 papers

Synthesis and properties of benzo[b]thiopheno[2,3-d]-1,3,2λ⁵-diazaphosphinane-2-thione derivatives

D. B. Nilov^a, V. G. Granik^b

^a Centre for Medicinal Chemistry. Sergo Ordzhonikidze All-Russian Research Chemical-Pharmaceutical Institute, Moscow, Russian Federation
^b Russian Research Centre 'Research Institute of Organic Intermediates and Dyes', Moscow, Russian Federation

Abstract: The treatment of 2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylic acid amide with phosphorus pentasulfide in the presence of pyridine yielded 4,5,6,7-tetrahydrobenzo[b]thiopheno[2,3-d]-1,3,2λ⁵-diazaphosphinane-2-thione; the alkylation of its sodium salts was studied.

Language: English

DOI: 10.1070/MC2003v013n02ABEH001705