E. V. Kudrik, E. M. Bauer, C. Ercolani, A. Chiesi-Villa, C. Rizzoli, A. A. Gaberkorn, P. A. Stuzhin, “Unsymmetrical porphyrazines with annulated 1,2,5-thia(seleno)diazole and 3,6-diamyloxybenzene rings: synthesis, characterization and X-ray crystal structure of H2{XN2}{3,6-(OAm)2Bz}3Pz (X = S, Se)”, Mendeleev Commun., 2001, Volume 11, Issue 2,Pages 45

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Unsymmetrical porphyrazines with annulated 1,2,5-thia(seleno)diazole and 3,6-diamyloxybenzene rings: synthesis, characterization and X-ray crystal structure of H₂{XN₂}{3,6-(OAm)₂Bz}₃Pz (X = S, Se)

E. V. Kudrik^a, E. M. Bauer^b, C. Ercolani^b, A. Chiesi-Villa^b, C. Rizzoli^c, A. A. Gaberkorn^a, P. A. Stuzhin^a

^a Department of Organic Chemistry, Ivanovo State University of Chemical Technology, Ivanovo, Russian Federation
^b Dipartimento di Chimica, Universita degli Studi di Roma 'La Sapienza', Roma, Italy
^c Dipartimento di Chimica Generale ed Inorganica, Universita di Parma, Italy

Abstract: Cyclotetramerization of a mixture of 3,4-dicyano-1,2,5-thiadiazole or 3,4-dicyano-1,2,5-selenodiazole with 3,6-diamyloxyphthalodinitrile gives new unsymmetrical porphyrazines with annulated 1,2,5-thia(seleno)diazole and 3,6-diamyloxybenzene rings; the structures of the 1:3 products H₂{XN₂}{3,6-(OAm)₂Bz}₃Pz (X = S, Se) has been elucidated by single-crystal X-ray diffraction.

Language: English

DOI: 10.1070/MC2001v011n02ABEH001372