O. E. Nasakin, V. P. Sheverdov, O. V. Ershov, I. V. Moiseeva, A. N. Lushchikov, V. N. Khrustalev, M. Yu. Antipin, “Single-stage synthesis of 3-amino-1,2-dicyano-4,6-diazabicyclo[3,2,1]oct-2-en-7-ones from β,β,γ,γ-tetracyanoalkanones”, Mendeleev Commun., 1997, Volume 7, Issue 3,Pages <nobr>112–113</nobr>

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Mendeleev Commun., 1997 Volume 7, Issue 3, Pages 112–113 (Mi mendc4810)

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Single-stage synthesis of 3-amino-1,2-dicyano-4,6-diazabicyclo[3,2,1]oct-2-en-7-ones from β,β,γ,γ-tetracyanoalkanones

O. E. Nasakin^a, V. P. Sheverdov^a, O. V. Ershov^a, I. V. Moiseeva^a, A. N. Lushchikov^a, V. N. Khrustalev^b, M. Yu. Antipin^b

^a Department of Chemistry, I.N. Ulyanov Chuvash State University, Cheboksary, Russian Federation
^b A.N. Nesmeyanov Institute of Organoelement Compounds of Russian Academy of Sciences, Moscow, Russian Federation

Abstract: The interaction of β,β,γ,γ-tetracyanoalkanones with aqueous ammonia leads to 3-amino-1,2-dicyano-4,6-diazabicyclo[3,2,1]oct- 2-en-7-ones; their structure has been established by X-ray crystallography.

Language: English

DOI: 10.1070/MC1997v007n03ABEH000722

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