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Pisma v Zhurnal Tekhnicheskoi Fiziki, 2020 Volume 46, Issue 18, Pages 45–48 (Mi pjtf4996)

Investigation of the mechanisms of compaction of CoSb$_{3}$ skutterudite nanopowders under field-activated sintering

A. S. Tukmakovaa, D. B. Shcheglovaa, A. P. Novitskiib, A. I. Voroninb, V. V. Khovailobc, A. V. Novotelnovaa

a St. Petersburg National Research University of Information Technologies, Mechanics and Optics
b National University of Science and Technology «MISIS», Moscow
c South Ural State University, Chelyabinsk

Abstract: We calculated the compaction parameters of CoSb$_{3}$ thermoelectric powders under field-activated sintering. The values of the creep activation energy, sensitivity to the strain rate, and the complex parameter of the material characterizing the state are obtained. The compaction of the powders is due to the mechanisms of grain sliding in the sample. We performed the computer simulation of the sintering process by the finite element method. The change in the dimensions of the sample is calculated using the creep deformation model. The simulation results correspond to the experimental data.

Keywords: spark plasma sintering, field-assisted sintering, simulation of powders densification, sintering kinetics, skutterudites, thermoelectrics.

Received: 20.03.2020
Revised: 23.06.2020
Accepted: 23.06.2020

DOI: 10.21883/PJTF.2020.18.50003.18296


 English version:
Technical Physics Letters, 2020, 46:9, 931–934

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