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Pisma v Zhurnal Tekhnicheskoi Fiziki, 2020 Volume 46, Issue 8, Pages 36–39 (Mi pjtf5132)

Decreasing density of grown-in dislocations in AlN/$c$-sapphire templates grown by plasma-activated molecular beam epitaxy

V. V. Ratnikov, D. V. Nechaev, A. V. Myasoedov, O. A. Koshelev, V. N. Zhmerik

Ioffe Institute, St. Petersburg

Abstract: Multiple-crystal X-ray diffraction and a multi-beam optical stress sensor were used to study AlN/$c$-sapphire templates grown by plasma-assisted molecular beam epitaxy. The influence of the nucleation and buffer layers growth regimes, temperature, the ratio between Al and N* growth fluxes on the stress generation and the character of the dislocation structure were analyzed. Templates with the best crystal quality with screw and edge threading dislocation densities in a range of 4 $\cdot$ 10$^{8}$ è 8 $\cdot$ 10$^{9}$ cm$^{-2}$, respectively, were obtained at the flux ratio of Al to N$^*$ close to 1 by using two-stage temperature regimes.

Keywords: molecular beam epitaxy, AlN/c-sapphire templates, threading dislocations, X-ray diffraction.

Received: 27.12.2019
Revised: 28.01.2020
Accepted: 28.01.2020

DOI: 10.21883/PJTF.2020.08.49307.18168


 English version:
Technical Physics Letters, 2020, 46:4, 389–392

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© Steklov Math. Inst. of RAS, 2024