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Pisma v Zhurnal Tekhnicheskoi Fiziki, 2024 Volume 50, Issue 3, Pages 31–35 (Mi pjtf6601)

Synthesis of MgAl$_2$O$_4$ thin films by Al and Mg anodic evaporation in a low-pressure arc (Ar/O$_2$, 1 Pa)

N. V. Gavrilov, D. R. Emlin, A. I. Medvedev

Institute of Electrophysics, Ural Branch, Russian Academy of Sciences, Yekaterinburg, Russia

Abstract: Films of magnesium aluminate spinel were synthesized by reactive anodic evaporation of Al and Mg in a low- pressure arc (Ar/O$_2$, 1 Pa) with vapor condensation at low temperature ($\sim$400$^\circ$C). Film deposition was assisted by ion flux 25–100 eV, 1–2 mA/cm$^2$) with a significant content of metal ions. Cubic spinel films had a strong texture (100) and microstrains of the crystal lattice are of $\sim$1%. The deposition rate of films was 1–3 $\mu$m/h at controlling of a relative content of Al and Mg atoms within 1.2–2.4.

Keywords: anodic evaporation, ionic assistance, magnesium aluminate spinel, self-heating cathode, thin films.

Received: 11.07.2023
Revised: 20.10.2023
Accepted: 09.11.2023

DOI: 10.61011/PJTF.2024.03.57041.19681



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© Steklov Math. Inst. of RAS, 2025