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Pisma v Zhurnal Tekhnicheskoi Fiziki, 2024 Volume 50, Issue 12, Pages 16–19 (Mi pjtf6695)

Synthesis of micro-sized powders of molybdenum borides by atmospheric AC arc discharge

Yu. Z. Vassilyeva, A. Ya. Pak, M. Yu. Speranskiy, A. A. Lavrenchuk, Yu. A. Neklya

Tomsk Polytechnic University, Tomsk, Russia

Abstract: The results of experimental studies proving the possibility of synthesis of molybdenum borides crystalline phases by atmospheric AC arc discharge are presented. According to X-ray diffractometry, there are four crystalline phases Ìî$_2$Â, ÌîÂ, ÌîÂ$_2$ è Ìî$_2$Â$_5$ in powder products obtained at different atomic ratios of molybdenum and boron. According to scanning electron microscopy data, molybdenum boride particles are characterized by a wide size distribution from 10 $\mu$m to 100 $\mu$m forming agglomerates with sizes up to $\sim$550 $\mu$m.

Keywords: molybdenum boride, arc discharge, alternating current, vacuum-free method.

Received: 12.12.2023
Revised: 09.03.2024
Accepted: 10.03.2024

DOI: 10.61011/PJTF.2024.12.58058.19838



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