M. M. Krayushkin, S. N. Ivanov, B. V. Lichitsky, D. V. Kozhinov, L. G. Vorontsova, Z. A. Starikova, A. A. Dudinov, “New synthesis of 4,5-diaryl-1,3-oxathiol-2-ones”, Mendeleev Commun., 14:2 (2004), 71

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New synthesis of 4,5-diaryl-1,3-oxathiol-2-ones

M. M. Krayushkin^a, S. N. Ivanov^a, B. V. Lichitsky^a, D. V. Kozhinov^a, L. G. Vorontsova^a, Z. A. Starikova^b, A. A. Dudinov^a

^a N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation
^b A.N. Nesmeyanov Institute of Organoelement Compounds of Russian Academy of Sciences, Moscow, Russian Federation

Аннотация: A new method for the synthesis of 4,5-diaryl-1,3-oxathiol-2-ones by the reaction of 2-hydroxyethanone derivatives with 1,1’-thiocarbonyldiimidazole is proposed. The structure of 4,5-bis(4-methoxyphenyl)-1,3-oxathiol-2-one was studied by X-ray diffraction.

Язык публикации: английский

DOI: 10.1070/MC2004v014n02ABEH001902