M. G. Vinogradov, D. V. Kurilov, G. V. Chel'tsova, V. A. Ferapontov, G. Heise, “Efficient resolution of (±)-α-cyclopropylethanol by crystallization of its inclusion complex with chiral diols”, Mendeleev Commun., 13:3 (2003), 124

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Efficient resolution of (±)-α-cyclopropylethanol by crystallization of its inclusion complex with chiral diols

M. G. Vinogradov^a, D. V. Kurilov^a, G. V. Chel'tsova^a, V. A. Ferapontov^a, G. Heise^b

^a N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation
^b Cambrex Corporation, East Rutherford, NJ, USA

Аннотация: The two-step inclusion crystallization of the chiral diol TADDOL with α-cyclopropylethanol has been found to allow resolving the racemic alcohol to yield (R)- or (S)-enantiomer (>98 % ee)

Язык публикации: английский

DOI: 10.1070/MC2003v013n03ABEH001757