S. I. Gorbin, A. A. Bakibaev, D. A. Kurgachev, V. S. Malkov, K. Yu. Novolokov, G. O. Sysoev, “Synthesis of 1-[1-(diphenoxyphosphoryl)alkyl]-3,4,6-trimethylglycolurils”, Mendeleev Commun., 33:5 (2023), 638

Эта публикация цитируется в 3 статьях

Communications

Synthesis of 1-[1-(diphenoxyphosphoryl)alkyl]-3,4,6-trimethylglycolurils

S. I. Gorbin, A. A. Bakibaev, D. A. Kurgachev, V. S. Malkov, K. Yu. Novolokov, G. O. Sysoev

Department of Chemistry, National Research Tomsk State University, Tomsk, Russian Federation

Аннотация: The reaction of 1,3,4-trimethylglycoluril, aliphatic aldehydes and triphenyl phosphite in the presence of methanesulfonic acid affords new phosphorus-containing derivatives of glycoluril. The thus formed diastereomers of 1-[1-(diphenoxy-phosphoryl)alkyl]-3,4,6-trimethylglycolurils were separated by reverse-phase HPLC

Ключевые слова: 1,3,4-trimethylglycolurils, phosphonates, diastereomers, Birum-Oleksyszyn reaction, triphenyl phosphite, one-pot synthesis.

Язык публикации: английский

DOI: 10.1016/j.mencom.2023.09.015

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